Ph3SnH Ph2SnH2 PhSnH3 SnPCV complex ecglccolorimetry

Possible degradation

Analysis

Gas-liquid chromatography was performed on a dual-column-dualdetector Varian Model 2400 instrument equipped, on one side, with a flame ionization detector and 0.7m x 2mm (i.d.) glass column containing 3% OV-17 on 60-80 mesh Gas Chrom Q. Column, injector and detector temperatures were 265, 275 and 300°C, respectively; the carrier gas was nitrogen. Tetraphenyltin eluted within 8min under those conditions. The second side of the chromatograph was equipped with a tritium electron-capture detector and a 1.1m x 2mm

Table 12.6 Method sensitivity

Minimum detectable Method sensitivity Species Method amount (vgmL~')a

Table 12.6 Method sensitivity

Minimum detectable Method sensitivity Species Method amount (vgmL~')a

Ptl4Sn

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